7RUR

Crystal structure of the hexadecameric form of Rv3208A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	120
Detector technology	PIXEL
Collection date	2017-03-08
Detector	DECTRIS PILATUS 2M
Wavelength(s)	0.98
Spacegroup name	I 4
Unit cell lengths	86.098, 86.098, 70.747
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.050 - 1.800
R-factor	0.2112
Rwork	0.210
R-free	0.23870
Structure solution method	AB INITIO PHASING
RMSD bond length	0.011
RMSD bond angle	1.333
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SHELX
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.050	1.864
High resolution limit [Å]	1.800	1.800
Rmerge	0.088
Number of reflections	23977	2364
<I/σ(I)>	26.05
Completeness [%]	100.0
Redundancy	9
CC(1/2)	0.997	0.909

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		290	8% Tacsimate (pH 4), 20 % PEG 3350