7QVZ

ARUK3001043_Notum

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-04-08
Detector	DECTRIS EIGER2 XE 16M
Wavelength(s)	0.9795
Spacegroup name	P 21 21 21
Unit cell lengths	60.152, 71.546, 78.371
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.840 - 1.470
R-factor	0.1732
Rwork	0.171
R-free	0.21710
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4uzq
Data reduction software	xia2
Data scaling software	xia2
Phasing software	MOLREP
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	78.370	1.500
High resolution limit [Å]	1.470	1.470
Number of reflections	58282	2831
<I/σ(I)>	12.4
Completeness [%]	100.0
Redundancy	13
CC(1/2)	1.000	0.430

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	4.2	296	1.5 M Ammonium Sulphate 0.1 M Sodium Citrate, pH4.2