Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-02-07 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1.00000 |
| Spacegroup name | P 63 |
| Unit cell lengths | 154.010, 154.010, 207.720 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.990 - 3.210 |
| Rwork | 0.228 |
| R-free | 0.25720 |
| Structure solution method | MIR |
| RMSD bond length | 0.002 |
| RMSD bond angle | 1.020 |
| Data reduction software | XDS (2021-04) |
| Data scaling software | XSCALE (2021-02) |
| Phasing software | PHASER (2.1.2) |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.990 | 3.290 |
| High resolution limit [Å] | 3.210 | 3.210 |
| Number of reflections | 45535 | 3341 |
| <I/σ(I)> | 15.57 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 20 | 20 |
| CC(1/2) | 0.990 | 0.510 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 285 | 15% PEG 1000, 6 mM hexaamminecobalt (III) chloride, 0.1 M tris/HCl |
