Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9779 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 96.180, 96.180, 153.760 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.100 |
R-factor | 0.18 |
Rwork | 0.178 |
R-free | 0.21640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7qc3 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.107 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.200 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.077 | 0.549 |
Number of reflections | 24601 | 3170 |
<I/σ(I)> | 18.3 | 4.6 |
Completeness [%] | 97.5 | |
Redundancy | 10.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.3 | 292 | 100 mM TRIS, 23% PEG 3350 |