Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-10-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 77.033, 84.539, 77.673 |
| Unit cell angles | 90.00, 113.59, 90.00 |
Refinement procedure
| Resolution | 51.390 - 1.434 |
| Rwork | 0.167 |
| R-free | 0.19860 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2ixi |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.453 |
| Data reduction software | XDS |
| Data scaling software | STARANISO |
| Phasing software | MoRDa |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.390 | 1.605 |
| High resolution limit [Å] | 1.434 | 1.434 |
| Number of reflections | 54843 | 2742 |
| <I/σ(I)> | 12.5 | |
| Completeness [%] | 65.9 | |
| Redundancy | 3.3 | |
| CC(1/2) | 0.999 | 0.585 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 291 | 1.0 M sodium citrate tribasic dihydrate, 0.1 M sodium cacodylate pH 6.5) Crystal was soaked in 15% w/v of D-xylose |
