7PU8
CARM1 in complex with EML980
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-08 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 75.207, 98.812, 208.401 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.070 - 2.190 |
R-factor | 0.1958 |
Rwork | 0.194 |
R-free | 0.22910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ih3 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.070 | 2.230 |
High resolution limit [Å] | 2.190 | 2.190 |
Rmerge | 0.100 | 1.599 |
Rmeas | 0.104 | 1.678 |
Rpim | 0.028 | 0.492 |
Number of reflections | 80189 | 3738 |
<I/σ(I)> | 14.4 | 1.3 |
Completeness [%] | 98.7 | 81.5 |
Redundancy | 13.4 | 10.7 |
CC(1/2) | 0.999 | 0.543 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 15% PEG 2000, 0.1M Sodium Chloride, 0.1M Tris HCl |