Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-01-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.88 |
| Spacegroup name | P 63 |
| Unit cell lengths | 90.337, 90.337, 76.650 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.441 - 1.400 |
| Rwork | 0.131 |
| R-free | 0.17830 |
| Structure solution method | MIRAS |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.793 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.400 | 1.480 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Rmerge | 0.064 | 0.670 |
| Rmeas | 0.069 | 0.850 |
| Number of reflections | 68251 | 9588 |
| <I/σ(I)> | 6.1 | 1.1 |
| Completeness [%] | 99.1 | 94.1 |
| Redundancy | 5.4 | 2.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 0.1M MES pH 6.0, 1.4-1.6M MgSO4 |
