Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 293 |
| Detector technology | PIXEL |
| Collection date | 2019-09-24 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.976246 |
| Spacegroup name | P 1 |
| Unit cell lengths | 69.335, 103.959, 170.127 |
| Unit cell angles | 92.27, 97.71, 106.40 |
Refinement procedure
| Resolution | 99.400 - 2.050 |
| Rwork | 0.223 |
| R-free | 0.25830 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6t7g |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.437 |
| Data reduction software | DIALS |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 99.597 | 2.090 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Number of reflections | 277094 | 13602 |
| <I/σ(I)> | 3.2 | 0.9 |
| Completeness [%] | 98.1 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.980 | 0.655 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M ammonium tartrate pH 7.0, 13 % PEG 3350 |
