Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2021-04-25 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.976284 |
| Spacegroup name | P 1 |
| Unit cell lengths | 69.452, 104.426, 170.781 |
| Unit cell angles | 92.29, 97.35, 106.55 |
Refinement procedure
| Resolution | 65.870 - 1.760 |
| Rwork | 0.231 |
| R-free | 0.26090 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6t7g |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.422 |
| Data reduction software | DIALS |
| Data scaling software | xia2 |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 65.870 | 1.790 |
| High resolution limit [Å] | 1.760 | 1.760 |
| Number of reflections | 438305 | 21409 |
| <I/σ(I)> | 7.6 | |
| Completeness [%] | 97.2 | |
| Redundancy | 3.1 | |
| CC(1/2) | 0.994 | 0.302 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Ammonium tartrate pH 6.5 , 14 % PEG 3,350 |
