Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-08-20 |
| Detector | RIGAKU SATURN A200 |
| Wavelength(s) | 1.542 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 142.010, 64.750, 116.380 |
| Unit cell angles | 90.00, 103.39, 90.00 |
Refinement procedure
| Resolution | 31.127 - 1.950 |
| Rwork | 0.239 |
| R-free | 0.28930 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | Internal Model |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.665 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 31.130 | 1.990 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.139 | 1.319 |
| Number of reflections | 75151 | 4003 |
| <I/σ(I)> | 6.2 | |
| Completeness [%] | 99.2 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | ethylene glycol per PEG 8000, carboxylic acids mix, buffer system 2, |
