7OHH
SaFtsZ complexed with GDP and BeF3-
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 71.750, 51.060, 87.840 |
Unit cell angles | 90.00, 111.03, 90.00 |
Refinement procedure
Resolution | 40.990 - 1.450 |
R-factor | 0.1789 |
Rwork | 0.177 |
R-free | 0.20730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rvn |
RMSD bond length | 0.009 |
RMSD bond angle | 1.182 |
Data reduction software | XDS (1.18.2_3874) |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.990 | 1.502 |
High resolution limit [Å] | 1.450 | 1.450 |
Number of reflections | 51784 | 5181 |
<I/σ(I)> | 12.83 | |
Completeness [%] | 98.1 | |
Redundancy | 3.9 | |
CC(1/2) | 0.998 | 0.306 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Tris-HCl pH 8.8, 28% PEG 5000 MME |