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7OG7

Crystal structure of the copper chaperone NosL from Shewanella denitrificans

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2016-02-08
DetectorDECTRIS EIGER X 16M
Wavelength(s)1.28096
Spacegroup nameF 41 3 2
Unit cell lengths179.066, 179.066, 179.066
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution44.767 - 1.850
R-factor0.1954
Rwork0.194
R-free0.22160
Structure solution methodSAD
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwareAutoSol
Refinement softwarePHENIX (1.13_2998)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.7701.890
High resolution limit [Å]1.8501.850
Number of reflections215861322
<I/σ(I)>35.3
Completeness [%]100.0
Redundancy76.6
CC(1/2)1.0000.431
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2930.1 M HEPES buffer at pH 7.5 and 1.4 M trisodium citrate tribasic dihydrate

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