7N2K

MicroED structure of sequence variant of repeat segment of the yeast prion New1p phased by ARCIMBOLDO-BORGES

Experimental procedure

Spacegroup name	P 31
Unit cell lengths	27.200, 27.200, 4.830
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	13.600 - 1.301
R-factor	0.1643
Rwork	0.161
R-free	0.18540
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	PHENIX

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	13.600	13.600	1.190
High resolution limit [Å]	1.100	1.880	1.100
Rmerge	0.211	0.192	0.483
Rmeas	0.226	0.204	0.601
Total number of observations	7893
Number of reflections	1357	335	191
<I/σ(I)>	4.92	8.86	1.21
Completeness [%]	83.4	99.4	53.2
Redundancy	5.817	7.899	2.257
CC(1/2)	0.985	0.982	0.604

Crystallization Conditions

crystal ID	method	pH	temperature	details
1