7N2G

MicroED structure of human CPEB3 segment(154-161) kinked polymorph phased by ARCIMBOLDO-BORGES

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	4.820, 20.480, 45.610
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.619 - 1.201
R-factor	0.1973
Rwork	0.192
R-free	0.23650
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	PHENIX

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	7.619	7.619	1.140
High resolution limit [Å]	1.100	4.260	1.100
Rmerge	0.192	0.120	0.697
Rmeas	0.223	0.137	0.804
Total number of observations	5536
Number of reflections	1453	28	145
<I/σ(I)>	4.29	8.02	1.41
Completeness [%]	66.9	53.8	68.4
Redundancy	3.81	3.571	3.821
CC(1/2)	0.980	0.980	0.533

Crystallization Conditions

crystal ID	method	pH	temperature	details
1