7N2F

MicroED structure of human CPEB3 segment (154-161) straight polymorph phased by ARCIMBOLDO-BORGES

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	4.830, 16.290, 29.020
Unit cell angles	90.00, 94.61, 90.00

Refinement procedure

Resolution	7.097 - 1.200
R-factor	0.2048
Rwork	0.202
R-free	0.23250
Data scaling software	XSCALE
Refinement software	PHENIX (1.16_3549)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	7.097	7.097	1.260
High resolution limit [Å]	1.200	3.980	1.200
Rmerge	0.144	0.120	0.187
Rmeas	0.159	0.130	0.209
Total number of observations	6430
Number of reflections	1130	30	145
<I/σ(I)>	8.31	11.96	5.9
Completeness [%]	78.7	63.8	79.2
Redundancy	5.69	6.433	5.09
CC(1/2)	0.981	0.975	0.976

Crystallization Conditions

crystal ID	method	pH	temperature	details
1