7MU0

MtbEttA in the ADP bound state

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	120
Detector technology	CCD
Collection date	2019-07-20
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.03
Spacegroup name	P 2 21 21
Unit cell lengths	50.060, 106.960, 269.190
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.060 - 2.900
R-factor	0.2026
Rwork	0.200
R-free	0.24580
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4fin
RMSD bond length	0.003
RMSD bond angle	0.737
Refinement software	PHENIX (0.9)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.060	3.004
High resolution limit [Å]	2.900	2.900
Number of reflections	33131	3255
<I/σ(I)>	8.16
Completeness [%]	99.8
Redundancy	2
CC(1/2)	0.997	0.553

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	0.1M MES, 0.2M MgCl2, 10% PEG 4000