Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-07-02 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9744 |
| Spacegroup name | F 41 3 2 |
| Unit cell lengths | 219.901, 219.901, 219.901 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.870 - 2.150 |
| R-factor | 0.1771 |
| Rwork | 0.175 |
| R-free | 0.21660 |
| Structure solution method | SAD |
| RMSD bond length | 0.001 |
| RMSD bond angle | 0.416 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX (1.18rc4_3812) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.190 |
| High resolution limit [Å] | 2.150 | 2.150 |
| Rmerge | 0.079 | 0.764 |
| Number of reflections | 25312 | 1238 |
| <I/σ(I)> | 33.64 | 3.1 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 11.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.9 | 297 | 20 % PEG 3350, 0.2 M Magnesium Formate, pH 5.9 |
