Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2018-01-26 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 69.200, 69.200, 49.200 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.030 - 1.650 |
| R-factor | 0.1809 |
| Rwork | 0.180 |
| R-free | 0.18970 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | SWISS-MODELLER MODEL |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.874 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 59.930 | 1.580 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Rmerge | 0.033 | 0.501 |
| Number of reflections | 18361 | 298 |
| <I/σ(I)> | 34.9 | 1.5 |
| Completeness [%] | 91.3 | 30.4 |
| Redundancy | 8.9 | 2.2 |
| CC(1/2) | 1.000 | 0.531 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | 12% PEG 8000, 100 mM MES pH 6.0 |
