Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-12-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9793 |
| Spacegroup name | C 2 2 2 |
| Unit cell lengths | 60.500, 115.720, 53.090 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 53.649 - 1.500 |
| R-factor | 0.189734709652 |
| Rwork | 0.189 |
| R-free | 0.21310 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.924 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | SHELXDE |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 53.649 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Number of reflections | 29976 | 1256 |
| <I/σ(I)> | 16 | |
| Completeness [%] | 99.3 | 99.6 |
| Redundancy | 4.3 | |
| CC(1/2) | 1.000 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 300 | 10-15% PEG 3350 and 0.2-0.25 M magnesium formate |
