7K6V
Crystal Structure of Virus-like Particles of GII.4 Norovirus Houston virus (HOV)
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-11-29 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9794806 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 420.170, 446.597, 463.952 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 3.000 |
| R-factor | 0.2088 |
| Rwork | 0.207 |
| R-free | 0.24180 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ihm |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.770 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 3.050 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.136 | 0.813 |
| Rmeas | 0.163 | |
| Rpim | 0.630 | |
| Number of reflections | 841777 | 38566 |
| <I/σ(I)> | 7 | 1 |
| Completeness [%] | 98.4 | 90.5 |
| Redundancy | 3.2 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 0.1 M Na Acetate pH 4.6, 0.1 M Cadmium Chloride, 30% PEG 400 |
