7HLF
PanDDA analysis group deposition -- Crystal Structure of TRIM21 in complex with Z2092555279
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-05-22 |
| Detector | DECTRIS EIGER2 XE 9M |
| Wavelength(s) | 0.92124 |
| Spacegroup name | I 4 |
| Unit cell lengths | 95.860, 95.860, 45.674 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.280 - 1.390 |
| R-factor | 0.1839 |
| Rwork | 0.183 |
| R-free | 0.20380 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.700 |
| Data reduction software | XDS |
| Data scaling software | Aimless (0.7.7) |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 31.250 | 31.250 | 1.410 |
| High resolution limit [Å] | 1.390 | 7.610 | 1.390 |
| Rmerge | 0.112 | 0.082 | 2.593 |
| Rmeas | 0.117 | 0.086 | 2.766 |
| Rpim | 0.032 | 0.025 | 0.953 |
| Total number of observations | 519108 | 3289 | 17033 |
| Number of reflections | 41853 | 275 | 2066 |
| <I/σ(I)> | 10.1 | 51.5 | 0.3 |
| Completeness [%] | 100.0 | 98.9 | 99.2 |
| Redundancy | 12.4 | 12 | 8.2 |
| CC(1/2) | 0.999 | 0.997 | 0.329 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 4 % PEG 400, 2 M AmmSO4, 0.1 M HEPES pH 8 |
