7FFR

Human Serum Albumin_2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97915
Spacegroup name	P 1 21 1
Unit cell lengths	57.981, 87.603, 59.619
Unit cell angles	90.00, 103.08, 90.00

Refinement procedure

Resolution	19.780 - 2.310
R-factor	0.2323
Rwork	0.230
R-free	0.25910
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6m4r
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.780	2.400
High resolution limit [Å]	2.310	2.310
Rmerge	0.065	0.463
Number of reflections	24015	2532
<I/σ(I)>	9.1
Completeness [%]	94.4
Redundancy	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG