Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-12-09 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 45.429, 50.443, 64.742 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 22.051 - 1.847 |
| R-factor | 0.19967210604 |
| Rwork | 0.199 |
| R-free | 0.22029 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.969 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 22.051 | 1.920 |
| High resolution limit [Å] | 1.846 | 1.850 |
| Rmerge | 0.084 | 0.642 |
| Rmeas | 0.088 | 0.677 |
| Rpim | 0.025 | |
| Number of reflections | 11611 | 1238 |
| <I/σ(I)> | 4.54 | |
| Completeness [%] | 99.3 | 94.6 |
| Redundancy | 11.9 | 9.3 |
| CC(1/2) | 1.000 | 0.917 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M sodium formate; 20% (w/v) PEG 3,350. |
