7F7P

AcrIIC4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	125
Detector technology	PIXEL
Collection date	2020-12-01
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.9795
Spacegroup name	P 1 21 1
Unit cell lengths	32.790, 52.110, 54.390
Unit cell angles	90.00, 95.69, 90.00

Refinement procedure

Resolution	29.260 - 2.030
R-factor	0.2285
Rwork	0.226
R-free	0.27920
Structure solution method	AB INITIO PHASING
RMSD bond length	0.007
RMSD bond angle	0.941
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.260	2.103
High resolution limit [Å]	2.030	2.030
Rmeas	0.097
Number of reflections	11895	1183
<I/σ(I)>	11.5
Completeness [%]	99.8
Redundancy	6.8
CC(1/2)		0.669

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	0.1 M CHES/Sodium hydroxide pH 9.5 30 % w/v PEG 3000