7EXX
The structure of DndG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97916 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 139.248, 182.286, 59.492 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.020 - 2.500 |
R-factor | 0.1682 |
Rwork | 0.166 |
R-free | 0.21360 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.198 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.073 | |
Number of reflections | 26349 | 2604 |
<I/σ(I)> | 17.6 | |
Completeness [%] | 98.6 | |
Redundancy | 3.3 | |
CC(1/2) | 0.777 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 287.15 | Sodium citrate tribasic |