7E76

The structure of chloroplastic TaPGI

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-04-18
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979
Spacegroup name	P 61
Unit cell lengths	73.387, 73.387, 360.262
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	47.660 - 2.650
R-factor	0.2072
Rwork	0.205
R-free	0.23790
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3ujh
RMSD bond length	0.004
RMSD bond angle	0.699
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.19.1_4122)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.660	2.700
High resolution limit [Å]	2.650	2.650
Rmerge	0.134
Number of reflections	29248	8
<I/σ(I)>	14.53
Completeness [%]	92.0
Redundancy	14.2
CC(1/2)		0.460

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	MES, PEG MME 2000