7E4D

Crystal structure of PlDBR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-17A
Synchrotron site	Photon Factory
Beamline	BL-17A
Temperature [K]	95
Detector technology	PIXEL
Collection date	2020-02-14
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.9
Spacegroup name	P 21 21 21
Unit cell lengths	64.461, 87.184, 117.573
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.740 - 2.600
R-factor	0.223
Rwork	0.221
R-free	0.26340
Structure solution method	SAD
RMSD bond length	0.002
RMSD bond angle	0.520
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.740	2.720
High resolution limit [Å]	2.600	2.600
Rmerge	0.084	1.028
Number of reflections	21068	2536
<I/σ(I)>	25.8
Completeness [%]	100.0
Redundancy	25.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG6000. HEPES, MPD