7DZJ

Fabp protein before hv

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-08-15
Detector	DECTRIS EIGER R 4M
Wavelength(s)	0.98
Spacegroup name	P 21 21 21
Unit cell lengths	56.688, 66.179, 68.076
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.680 - 1.630
R-factor	0.1884
Rwork	0.186
R-free	0.23080
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1lkk
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.450	1.720
High resolution limit [Å]	1.628	1.630
Rmerge	0.013	0.246
Number of reflections	28327	3195
<I/σ(I)>	22.4	2.6
Completeness [%]	100.0
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	277	0.1 M potassium thiocyanate, pH 7.0, 30% PEG 2000 monomethyl ether