7DYA

Crystal structure of TmFtn with calcium ions

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NFPSS BEAMLINE BL18U
Synchrotron site	NFPSS
Beamline	BL18U
Temperature [K]	100
Detector technology	CCD
Collection date	2020-07-17
Detector	RAYONIX MX-225
Wavelength(s)	0.979
Spacegroup name	H 3 2
Unit cell lengths	175.434, 175.434, 357.421
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	38.584 - 2.197
R-factor	0.1751
Rwork	0.175
R-free	0.20010
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1vlg
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.584	2.197
High resolution limit [Å]	2.197	2.197
Number of reflections	107433	10652
<I/σ(I)>	5.97
Completeness [%]	99.9
Redundancy	6.8
CC(1/2)	0.992	0.979

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	4.6	293	14% 2-Propanol, 70 mM Sodium acetate/ HCl pH 4.6, 140 mM Calcium chloride, 30% Glycerol