7DNF
DARPin 63_B7 in complex with V3-IY (MN) crown mimetic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.350, 105.980, 64.020 |
Unit cell angles | 90.00, 93.44, 90.00 |
Refinement procedure
Resolution | 48.260 - 1.780 |
R-factor | 0.188 |
Rwork | 0.187 |
R-free | 0.22540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1SVX chain A |
RMSD bond length | 0.004 |
RMSD bond angle | 0.548 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.260 | 1.844 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.128 | 1.572 |
Rmeas | 0.073 | |
Number of reflections | 59433 | 5571 |
<I/σ(I)> | 7.67 | |
Completeness [%] | 96.5 | 90.79 |
Redundancy | 3.9 | 3.6 |
CC(1/2) | 0.995 | 0.271 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 25% w/v PEG 3350, 0.2M (NH4)2SO4, 0.1M Bis-Tris pH 5.5 |