7CYA

Saimiri boliviensis boliviensis galectin-13 with lactose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-01-12
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.98
Spacegroup name	P 1 21 1
Unit cell lengths	33.529, 58.789, 40.833
Unit cell angles	90.00, 113.63, 90.00

Refinement procedure

Resolution	19.030 - 1.710
R-factor	0.1774
Rwork	0.174
R-free	0.20950
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6kjx
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.600	1.740
High resolution limit [Å]	1.710	1.710
Rmerge	0.055	0.545
Number of reflections	15714	835
<I/σ(I)>	10.4
Completeness [%]	99.5
Redundancy	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG