7CSG
AtPrR2 in apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-03-12 |
Detector | MAR555 FLAT PANEL |
Wavelength(s) | 0.9798 |
Spacegroup name | P 1 |
Unit cell lengths | 44.291, 57.936, 71.559 |
Unit cell angles | 107.32, 95.77, 113.24 |
Refinement procedure
Resolution | 34.161 - 1.997 |
R-factor | 0.191275975048 |
Rwork | 0.189 |
R-free | 0.23784 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qyd |
RMSD bond length | 0.007 |
RMSD bond angle | 0.802 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.162 | 2.070 |
High resolution limit [Å] | 1.996 | 2.000 |
Rmerge | 0.115 | 0.422 |
Number of reflections | 39962 | 3909 |
<I/σ(I)> | 24.3 | |
Completeness [%] | 97.6 | |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 0.2M magnesium chloride, 0.1 M sodium HEPES, pH 7.5, 25% PEG 3350 |