Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-13 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.97852 |
| Spacegroup name | P 3 |
| Unit cell lengths | 81.391, 81.391, 60.423 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 26.640 - 1.901 |
| Rwork | 0.171 |
| R-free | 0.18750 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4nek |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.262 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.000 | 1.969 |
| High resolution limit [Å] | 1.900 | 1.901 |
| Rmeas | 0.105 | 0.540 |
| Number of reflections | 35138 | 3505 |
| <I/σ(I)> | 23.61 | |
| Completeness [%] | 99.5 | 98.43 |
| Redundancy | 9.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 10% PEG6000, 0.1 M sodium citrate tribasic dehydrate pH 5.0 |
