7CP6
Crystal structure of FqzB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.005630 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.893, 120.181, 68.048 |
Unit cell angles | 90.00, 94.11, 90.00 |
Refinement procedure
Resolution | 41.640 - 2.200 |
R-factor | 0.2139 |
Rwork | 0.213 |
R-free | 0.23770 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.690 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.640 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.124 | 0.822 |
Number of reflections | 45285 | 4430 |
<I/σ(I)> | 14.87 | |
Completeness [%] | 99.7 | |
Redundancy | 13.6 | |
CC(1/2) | 0.997 | 0.837 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG3350, Bis-Tris propane, sodium iodide |