7CLU
PigF with SAH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-11-02 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 69.095, 52.358, 92.835 |
| Unit cell angles | 90.00, 97.35, 90.00 |
Refinement procedure
| Resolution | 19.570 - 1.900 |
| Rwork | 0.200 |
| R-free | 0.24800 |
| Structure solution method | SAD |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.684 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | CRANK2 |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.574 | 1.940 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rpim | 0.052 | 0.624 |
| Number of reflections | 48615 | 3366 |
| <I/σ(I)> | 7.9 | |
| Completeness [%] | 93.6 | |
| Redundancy | 2.2 | 2.1 |
| CC(1/2) | 0.996 | 0.506 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295 | MPD |
