7C96

Avr1d:GmPUB13 U-box

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2016-12-17
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9791
Spacegroup name	P 65 2 2
Unit cell lengths	69.547, 69.547, 153.480
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	28.760 - 2.510
R-factor	0.2365
Rwork	0.235
R-free	0.24920
Structure solution method	SAD
Data reduction software	XSCALE
Data scaling software	XSCALE
Phasing software	HKL2Map
Refinement software	PHENIX (1.18_3861)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	28.760	28.760	2.660
High resolution limit [Å]	2.510	7.320	2.510
Rmerge	0.079	0.043	0.970
Rmeas	0.083	0.045	1.027
Total number of observations	153546
Number of reflections	14060	529	2247
<I/σ(I)>	18.81	45.39	2.38
Completeness [%]	99.3	90.6	98.4
Redundancy	10.921	9.764	9.145
CC(1/2)	0.999	0.997	0.803

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277.15	BIENCE,PEG20,000,