7BVM

Crystal structure of lysozyme delivered in wheat starch

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 11C
Synchrotron site	PAL/PLS
Beamline	11C
Temperature [K]	298.15
Detector technology	PIXEL
Collection date	2019-06-11
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9795
Spacegroup name	P 43 21 2
Unit cell lengths	79.360, 79.360, 38.630
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	56.116 - 2.000
R-factor	0.189
Rwork	0.184
R-free	0.23330
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6ig6
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.15.2_3472)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	80.000	2.070
High resolution limit [Å]	2.000	2.000
Number of reflections	8796	840
<I/σ(I)>	4.06
Completeness [%]	100.0	100
Redundancy	124.5	1.58
CC(1/2)	0.964	0.635

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SMALL TUBES		293.5	sodium acetate, PEG 8000, NaCl