7BUX
Eucommia ulmoides FPS1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2017-11-09 |
| Detector | RAYONIX MX300HE |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 54.000, 71.270, 103.380 |
| Unit cell angles | 90.00, 103.50, 90.00 |
Refinement procedure
| Resolution | 35.840 - 2.200 |
| R-factor | 0.234 |
| Rwork | 0.233 |
| R-free | 0.24800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4kk2 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.884 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.840 | 2.279 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Number of reflections | 38428 | 29298 |
| <I/σ(I)> | 10.77 | |
| Completeness [%] | 98.7 | |
| Redundancy | 7.5 | |
| CC(1/2) | 0.995 | 0.837 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | HEPES, PEG 10000, Ethylene glycol, MgCl2 |
