7BUU
Eucommia ulmoides TPT3, crystal form 1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-11-06 |
| Detector | RAYONIX MX300HE |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 80.260, 80.260, 278.950 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.440 - 3.000 |
| R-factor | 0.2228 |
| Rwork | 0.222 |
| R-free | 0.23290 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4kk2 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.239 |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.440 | 3.107 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Number of reflections | 19181 | 1849 |
| <I/σ(I)> | 24.7 | |
| Completeness [%] | 99.9 | |
| Redundancy | 28.6 | |
| CC(1/2) | 1.000 | 0.790 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, DL-Malic acid, Risedronate, MgCl2 |
