7BDZ

X-ray structure of Hen Egg White Lysozyme with dirhodium tetraacetate (1)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Temperature [K]	100
Detector technology	CCD
Collection date	2016-07-13
Detector	RIGAKU SATURN 944
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	77.964, 77.964, 37.291
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.480 - 1.940
Rwork	0.156
R-free	0.21740
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	193l
RMSD bond length	0.009
RMSD bond angle	2.384
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.480	1.970
High resolution limit [Å]	1.940	1.940
Rmerge	0.095	0.440
Rpim	0.045	0.249
Number of reflections	8895	426
<I/σ(I)>	14.9	2.2
Completeness [%]	99.0
Redundancy	5.3
CC(1/2)	0.997	0.808

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	293	0.1M sodium acetate, 20% ethylene glicol, 0.6 M sodium nitrate