7BDZ
X-ray structure of Hen Egg White Lysozyme with dirhodium tetraacetate (1)
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-07-13 |
| Detector | RIGAKU SATURN 944 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 77.964, 77.964, 37.291 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.480 - 1.940 |
| Rwork | 0.156 |
| R-free | 0.21740 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 193l |
| RMSD bond length | 0.009 |
| RMSD bond angle | 2.384 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.480 | 1.970 |
| High resolution limit [Å] | 1.940 | 1.940 |
| Rmerge | 0.095 | 0.440 |
| Rpim | 0.045 | 0.249 |
| Number of reflections | 8895 | 426 |
| <I/σ(I)> | 14.9 | 2.2 |
| Completeness [%] | 99.0 | |
| Redundancy | 5.3 | |
| CC(1/2) | 0.997 | 0.808 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 293 | 0.1M sodium acetate, 20% ethylene glicol, 0.6 M sodium nitrate |
