Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-03-02 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.919762 |
| Spacegroup name | P 63 |
| Unit cell lengths | 75.890, 75.890, 177.670 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.900 - 2.430 |
| R-factor | 0.2378 |
| Rwork | 0.237 |
| R-free | 0.24610 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5m38 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.10.4 (11-DEC-2020)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.900 | 2.570 |
| High resolution limit [Å] | 2.430 | 2.430 |
| Number of reflections | 21834 | 3454 |
| <I/σ(I)> | 11.7 | |
| Completeness [%] | 99.7 | |
| Redundancy | 21.1 | |
| CC(1/2) | 0.991 | 0.777 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M MES, pH 5.5-6.5 0.6-1 M ammonium sulfate |
