7BAX
Crystal structure of LYS11 ectodomain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX IV BEAMLINE BioMAX |
| Synchrotron site | MAX IV |
| Beamline | BioMAX |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-02-22 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.954 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 114.940, 114.940, 59.150 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.080 - 2.900 |
| R-factor | 0.192 |
| Rwork | 0.188 |
| R-free | 0.22580 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7au7 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.100 |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.950 |
| High resolution limit [Å] | 2.880 | 2.880 |
| Rmeas | 0.088 | 0.472 |
| Number of reflections | 8086 | 60 |
| <I/σ(I)> | 15.97 | 4.93 |
| Completeness [%] | 77.1 | 7.7 |
| Redundancy | 9.7 | 7.8 |
| CC(1/2) | 0.999 | 0.897 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 0.1 M Sodium malonate pH 6.0, 12% PEG3350 |
