7B0E
Crystal structure of SmbA loop deletion mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-11-06 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.000 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 56.040, 56.040, 205.068 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.523 - 1.400 |
R-factor | 0.1494 |
Rwork | 0.148 |
R-free | 0.17730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6gs8 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.898 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.12-2829-000) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.530 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.098 | |
Rpim | 0.021 | |
Number of reflections | 65594 | 6381 |
<I/σ(I)> | 20.6 | 2.6 |
Completeness [%] | 99.9 | 99.87 |
Redundancy | 22.9 | 22.9 |
CC(1/2) | 0.990 | 0.780 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.2M CaCl2, 0.1M Tris pH 8.0, 20% w/v PEG 6000 |