7AW8
Alpha-actinin in Rhodamnia argentea
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-03 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.99988 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 37.219, 37.219, 290.266 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.380 - 1.500 |
R-factor | 0.1682 |
Rwork | 0.167 |
R-free | 0.19010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a36 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.380 | 48.380 | 1.530 |
High resolution limit [Å] | 1.500 | 8.220 | 1.500 |
Rmerge | 0.095 | 0.046 | 0.883 |
Rmeas | 0.098 | 0.048 | 0.911 |
Rpim | 0.023 | 0.012 | 0.222 |
Total number of observations | 4733 | 30482 | |
Number of reflections | 71951 | 334 | 1855 |
<I/σ(I)> | 15.5 | 37.2 | 2.9 |
Completeness [%] | 99.9 | 99.8 | 99.4 |
Redundancy | 18.5 | 14.2 | 16.4 |
CC(1/2) | 0.999 | 0.999 | 0.907 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 3.1 M NaFormate 0.1 M NaAcetate pH 4.5 |