7AW7
CCAAT-binding complex and HapX bound to Aspergillus nidulans cccA DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-07 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 76.150, 133.150, 199.790 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.000 | 3.500 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.058 | 0.527 |
Number of reflections | 14326 | 1166 |
<I/σ(I)> | 14.7 | 2.8 |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 5.2 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M ammonium fluoride, 20% PEG3350 |