Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-09-29 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.3051 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 95.160, 95.160, 52.510 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.000 - 2.855 |
| Rwork | 0.207 |
| R-free | 0.23400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7ath |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.782 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.000 | 3.030 |
| High resolution limit [Å] | 2.850 | 2.850 |
| Number of reflections | 10684 | 1700 |
| <I/σ(I)> | 12.2 | |
| Completeness [%] | 99.6 | |
| Redundancy | 14 | |
| CC(1/2) | 0.990 | 0.760 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | MES pH6 100mM, PEG6K 22%, Formamide 6%, ZnCl2 5-15mM |
