7ATH

Crystal structure of UipA

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-09-29
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.99987
Spacegroup name	P 43 21 2
Unit cell lengths	96.130, 96.130, 52.550
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.991 - 2.343
Rwork	0.218
R-free	0.24740
Structure solution method	SAD
RMSD bond length	0.011
RMSD bond angle	1.842
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHENIX
Refinement software	REFMAC (5.8.0257)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.000	2.330
High resolution limit [Å]	2.200	2.200
Number of reflections	23892	3813
<I/σ(I)>	17.5
Completeness [%]	99.8
Redundancy	14
CC(1/2)	0.990	0.530

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	MES pH6 100mM, PEG6K 22%, ZnCl2 5-15mM Formamide 6%