6O5K
Murine TRIM28 Bbox1 domain
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 33.012, 51.459, 72.884 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 42.040 - 1.600 |
R因子 | 0.18181 |
Rwork | 0.180 |
R-free | 0.20764 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.194 |
Data reduction software | XDS (Jan 10, 2014) |
Data scaling software | Aimless |
Phasing software | SHELXCD |
Refinement software | REFMAC (5.8.0230) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 42.040 | 1.630 |
分解能 [Å] (高) | 1.600 | 1.600 |
Rmerge_l_obs | 0.267 | 3.950 |
Rpim | 0.072 | 1.075 |
独立反射数 | 17060 | 817 |
<I/σ(I)> | 10.3 | 0.97 |
完全性 [%] | 100.0 | 100 |
冗長性 | 14.3 | 14.2 |
CC(1/2) | 0.997 | 0.391 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 6 | 291 | 2.7 M Ammonium sulfate, pH 6.0 |