6N6H
Vibrio cholerae Oligoribonuclease bound to pCpU
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.977 |
Spacegroup name | P 32 2 1 |
格子定数 [Å] | 89.070, 89.070, 60.143 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 35.791 - 1.757 |
R因子 | 0.1617 |
Rwork | 0.161 |
R-free | 0.18370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6n6a |
Data reduction software | XDS |
Data scaling software | SCALA (3.3.22) |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 47.430 | 47.430 | 1.850 |
分解能 [Å] (高) | 1.757 | 5.550 | 1.760 |
Rmerge_l_obs | 0.035 | 0.986 | |
Rmeas | 0.062 | 0.037 | 1.030 |
Rpim | 0.018 | 0.011 | 0.297 |
Total number of observations | 334350 | ||
独立反射数 | 27804 | 964 | 4001 |
<I/σ(I)> | 21.8 | 13.6 | 0.8 |
完全性 [%] | 99.9 | 99.9 | 99.6 |
冗長性 | 12 | 11.3 | 11.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M BisTris (pH 5.5), 17% polyethylene glycol 3350, and 20% xylitol |