6JXP
Room temperature structure of lysozyme delivered in LCP by serial millisecond crystallography
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 298.15 |
Detector technology | PIXEL |
Collection date | 2019-02-25 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97942 |
Spacegroup name | P 43 21 2 |
格子定数 [Å] | 78.410, 78.410, 37.930 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 55.440 - 1.560 |
R因子 | 0.1708 |
Rwork | 0.168 |
R-free | 0.20030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6irj |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.022 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 78.700 | 1.610 |
分解能 [Å] (高) | 1.560 | 1.560 |
独立反射数 | 17418 | 1685 |
<I/σ(I)> | 6 | 1.26 |
完全性 [%] | 99.9 | 99.23 |
冗長性 | 318.4 | |
CC(1/2) | 0.991 | 0.436 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | SMALL TUBES | 293.5 | sodium acetate, PEG 8000, NaCl |